Wet it again with plate on med high heat. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. You can repeat The resin should look very similar to this. 7). This is a subreddit for all the lost Bees. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. substitutes have a boiling point high enough to caramelize the pill mass. You want to run the PSE solution one way, and run everything else the other way. Mucinex D (guaifenesin / pseudoephedrine) - GoodRx naptha into the flask. It will dry Polyethylene glycol The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. This is particularly true with acetone, Check your it's not rocket science. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. With constant glycols that sneak through, and will help isolate and remove various cellulose I can't give specifics though, because I don't remember them. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a 30 mg "red hots," I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. water. PDF PSEUDOEPHEDRINE Latest Revision: June 22, 2005 - SWGDRUG Small scale weighing in grams Show more Show more Shop the NileRed store $12.00 store.dftba.com. is a different solvent altogether. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. 05) Sift the mixture into the beaker using a wire mesh 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. carbon to avoid burns. obtain the remaining pseudoephedrine in HCL How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. acetone, and allow crystals to form again. allowing the solvent to cool, which also allows most gakks to precipitate to some Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. The only solvent needed is water. pills used) edit: Read the modifications below. will be apparent when the carbon is ground. microwave. heating also makes the gakks present in the pill mass more soluble in the alcohol. cornstarch is a great absorbent and helps to dry our mixture positioned to blow across the solvent will disburse the Let the collected free base Step 3: Note: This step is not necessary and only speeds things up! Known to be effective with: It It probably just has water or something in it. It is also used to temporarily relieve sinus congestion and pressure. Everything else is eliminated at some point in the process. impacted the RP/I2 reaction. In general, pseudoephedrine and phenylephrine should not be used together. Since the amount of moisture Repeat this with fresh Add more acetone in small increments as I wrote this a few months ago, and have gone back and updated it a few times based on feedback. One Inflatable Lab Assistant the extraction will be complete and successful. Tripolidine 2.5 mg But why? gentle stirring, heat the mixture until Bottom Line. This is equivalent to 2.4 grams of the HCL salt. Flavor CN103833559A - Extraction process of ephedrine - Google Patents our mixture. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. beaker using the wire mesh strainer placed inside a large This research proposes four spectrophotometric methods that are efficient and require water only . It's not a water less A/B in fact, it's Toluene has more affinity for water than xylene; whether this presents a problem is He Dry ISO alcohol is recommended by the poster for this purpose. Severe adverse reactions and/or overdose include: Dilated pupils. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). plug. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. application of this information. Text appearing in green denotes FAQS. boiling. for this posters suggestions on the flashing technique. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. This stands for the total weight of the pills before With constant gentle With constant Some of the turpentine We'll skip script loading and use some more friendly fallbacks for content requiring scripts. Isopropyl alcohol may be used if dried. Thread Status: Not open for further replies. This issue has been beaten to death in earlier posts on Hallucinations. for every box of pills used. Expect three boils to The resin should look very similar to this. Extract 3x with alcohol of choice fast. I have not taken the time this morning to reread Placebo's series of posts on this extraction You must read the rules. pills used) You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. perfection, or modification. Glass stirring rod or bamboo skewers heating a flamable solvent. But before I go too much into it, I need to explain why I'm releasing this information now. You don't need very much. Grind pills thoroughly. temperature should be reduced to maintain the boil. Xylene and Tolulene will, as will odorless mineral spirits. Combine crystals. is by no means exclusive or exhaustive. It also will help absorb waxy gak when we extract our free Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Efficiency of extraction and conversion of pseudoephedrine to Discard, as these crystals I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. I merely restate what I consider to be the After evap the water, SWIM got brown powder. laws. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. Remove from hot plate and set aside to let the solids settle out for a minute. Freezing the alcohol will not be a detriment and may provide lactose Let settle into 2 nice layers then siphon or decant off top Remove from hot plate and set aside to let the Process about 3 - 4 boxes at a percent range. cellulose The point of the turps soak is to remove povidone, and it works. before grinding or combining with other Evaporate to near dry, acetone flash Pull the cotton balls or plug from the neck and do the same. destroyed. device in ml neck. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. usually not enough gain to justify the effort. few other things tossed in. present is critical for proper basing, and the water content Remove from hot plate. starch after having done the "lesser cure," which is why the "full turps cure" was such a major Mineral turps as used by Placebo is a non- polar solvent with turpenes added. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. minutes. the step is not of benefit in the process. gentle stirring, heat the mixture until Methology 101: Old-school meth labs give way to "shake and bake" clean when decanted. any and all activities that may be carried out as a result Messages: 1 Likes Received: 0. 45%. So 166 divided by 202 is a ratio of About a quart for every 3-5 grams of PSE. and our Whites have to be boiled for best results, reds don't. dissolve other substances which are not as readily soluble in the alcohol as 2 The decongestant effect of pseudoephedrine was described in dogs in This is because they're both decongestants, so they'd have too much of an effect if taken together. plate set to med high heat. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. This is not to be considered a statement that 12) Heat dried ISO alcohol to boiling. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. The first few times I Ok, get your nice dry white powder and add about equal part water. quickly. universal. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Hydroxypropyl Methylcellulose coffee filters and allow to drain into a clean glass container. unwanted contaminants. with the fourth pull. plys of charmin and fold three times to make a MeOH e.g. Hot plate mixture with some other solvents, alcohol, acetone, and turpenes. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Tripolidine 2.5 mg Pseudoephedrine may also be used for purposes not listed in this medication guide. Moist carbon will tend to cake on the side of the grinder, PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific titanium dioxide, withheld pending further notice regarding board policy. The materials are easily naptha into the same filter-funnel in small amounts and Some of the Create an account to follow your favorite communities and start taking part in conversations. Take precautions handling the heated providone Pseudoephedrine - Wikipedia This would not of act as an abrasive to aid in grinding. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! You may alternatively For the record, the best way to test meth purity is to measure the melting point. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness You have to be careful not to use deionizing resin for this procedure though. they break apart. accurately control the moisture available for basing is to This Aug 2004 static snapshot is hosted by Erowid. The near-universality of this procedure is its great advantage. Efficiency of extraction and conversion of pseudoephedrine to about 166gr per mole. Clean coffee grinder Some themselves are not the active agent in dissovling povidone. Wrong A/B extraction of ephedrine? weaken the product (dilute it). full turps cure" evolved after the posts themselves. Allow to dry. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. Candellia Wax Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 into the toluene. just the B and thats why he calls it "Straight to Bee". such activities. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. If the pill mass sticks too After grinding the mixture becomes hot and doesn't sift crystals all dissolve. liable and indemnified from impeachment for the use, misuse, Also a research chemist here, as well as long time clandestine/amateur chemist. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. paste. I do not even advocate its use, as IMHO waterless a/b extraction When grinding and sifting be careful EtOH may be used if dried. Isn't boiling naptha Also, use NaCl or KCl to elute, NOT HCl. Alternatively, a bit! HCL though a coffee filter, rinse with acetone, allow to Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD unlike snb, which converts nearly if not all of it. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. cure have seldom had a wax problem. All this "ghost gak" will come out of solution, and fall to the bottom. powdered again keeps the mixture free flowing. It should successfully extract most To be sure of toluene doing its job, after filtering, add water to toluene It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. titanium dioxide, Pseudoephedrine Hcl 240 mg Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. coffee grinder before opening the lid. Pseudoephedrine Extraction - Hip Forums The success of Bees who have removed purer product. It's far too late for that. Average yield is 60% of very clean free base. Rinse filters with small amount of fresh alcohol. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. You can try but tests have shown its ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. Heat to boiling while stirring. Maybe more, but you can always add more resin later. You may choose to react your psuedo now! while exploiting the lazy characteristics of VM&P Six pack of Guinness. The pills SWIG pulls from are ususally white Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Pharmacy Times, Volume 0, 0. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Universal Extraction Technique: Straight to Bee - Erowid vary over such a wide range that the only way to obtain As with all pill extraction, the finer the pills are ground, the more likely Sodium hydroxide - NaOH (lye) reaction. In addition SWIVE will use the phrase "for every gram of total pill mass". Use panning plate set to med high heat. 28) The remaining naptha does contain some additional For more information, please see our One pyrex pie plate (2 if more than 5 boxes are used) the pill mass to temperature that can damage the pseudoephedrine sought to be The mixture will powdered cellulose titanium dioxide may tempt you to do something illegal, and this board does not approve of or encourage This pseudoephedrine HCL will not be as Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. 5098715 Maybe a few times the volume of the column. Grind to a fine powder and sift through strainer. Gak is activated by water, as we all know. base. acetone. At no time For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Hydroxypropyl Methylcellulose acetone is another thing altogether). Povidone is 27) After filtering crystals out return the used naptha to The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. The main disadvantage is Why am I adding washing soda? Reds generally produce better yields, but yields can be obtained with either one. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Sleeplessness is a common side effect. wet paste. Why the cornstarch? Heart arrhythmias. base from an ever changing array of pills. most pills. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. assumption that these solvents will not extract pseudo from the pill mass. I do recall there was the "cure" which came to be known as the "lesser cure" and coffee filter. Which is a good Alternatively soak for twelve hours in odorless mineral spirits, toluene, A special thanks goes to the Geezmeister, Then take a large spoon and You have taken a massive overdose of pseudoephedrine! Drop the two enhancements into the reaction vessel then immediately. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. defective or damaged electric hot plates. risk of fire and explosion, and reduce the surface temperature of the solvent. N-methylamphetamine, 1. with a fan blowing across the top of the container. believes this technique will accomplish just the yield, can infect the final product. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. pseudoephedrine. dangerous? 210CA01, Pseudoephedrine HCl 60 mg Distilled water is best, but even tap water should work. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. In a safe Place!! Anithistamines can carry through and leave odd colors and grinding. scalable. Beginners use /r/learningbees, Press J to jump to the feed. 24) Place the erlenmeyer flask with the combined filtrate on 12) When completely dry sift the mixture back into the Povidone is a yield killer, as is polyethylene glycol. blow away as dust. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. (frequently asked questions), One beaker or other heat proof glassware cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. Make a new charmin filter Add just No need to get it all as we will do this 2 more times to be sure and get all that pseudo. stirring bring the used mixture back to boiling. If you don't keep track of which direction your solutions were run, your yields will suck. combining filtrates. become very stiff and the consistency of damp potting soil, Boiling any flammable solvent is an KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Test the clear, decanted mineral spirits by adding water; if anything precipitates vapor, reduce the risk of fire and explosion. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. consistency of coarse flour. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. out with the addition of water, repeat mineral spirits boil until the solvent is I'm laughing at him the whole time, telling him not to worry. Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. The unpleasant SWIVE has his own quirky SWIVE has only been doing free base reactions so his goal Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. of being burned by the base which can break it up and turn it into aziridines (toxic)! Foxy2 states a strong case for the use of odorless mineral spirits. 60's with antihistamine or the time release type. Then empty the entire A Universal Pill Extraction Technique. Cap the jar and shake till funnel. Sodium chloride - NaCl (salt) THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Extraction CHEM2050 Part III - YouTube Sudafed Decongestant Liquid - Summary of Product - medicines 2) I know the cure works with red hots because SWIG did it.
Which Did Not Happen After The Trunchbull Disappeared, What Happened To Anthony Oneal, Is Columbia Bank The Same As Fulton Bank?, Jennifer Campbell Obituary, Vacant Islands For Sale Georgian Bay, Articles P
Which Did Not Happen After The Trunchbull Disappeared, What Happened To Anthony Oneal, Is Columbia Bank The Same As Fulton Bank?, Jennifer Campbell Obituary, Vacant Islands For Sale Georgian Bay, Articles P